Scanning Reference Electrode technique

Description:

Scanning reference electrode technique (SRET) is an in situ technique used to study the electrochemical process during localized corrosion without interrupting the process taking place.

Within the electrolyte directly above a localized electrochemical active site, there exist an electromagnetic field. A probe consisted of two platinum wires can sense the potential difference between two different places where the two platinum wires are located. This potential difference then is processed by a differential amplifier. By scanning the SRET probe over the surface of the test material immersed in an electrolyte, these fields may be mapped out as a function of x and y or monitored with respect to time. Resulting data can be instantly display, stored and manipulated in a number of formats including individual linescans, area maps and sequential time related images.

The potential field distribution over the surface of the electrochemically active site is representative of the localized current flow. By using a calibration procedure the SRET can also be used to make discrete current measurements.

Technical details:
Maximum specimen size350 x 200 x 30 mm
Probe movementx = 100 mm
y = 100 mm
z = 35 mm
Scan speed1 - 25 mm/sec
Stepper motor resolution (steps per 360° revolution)1000
Maximum probe step resolution0.5 µm
Amplifier characteristics
 Input coupling
Gain
DC and AC
1x - 5000x (optional hi-gain headamp)
Electrolyte tank capacity4.5 litres
Computer
 Type
Harddisk
Floppy's
CD-writer
Printer
486DX2, 66MHz
80 Mb
3.5 inch 1.44 Mb
230 Mb
HP Deskjet 560C colour printer
Software
 Operating system
Image display
Data point resolution
Colour palette
Microsoft windows
Super VGA (800x600x32k colours
variable from 8x6 to 512x384
16,777,216

 
Room: 01.19

 
More Technical information: Techinfo@mtm.kuleuven.be
 

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Last modified: January, the 18th, 2002